Drug samples (600 mg) were placed in 25 mL stainless steel jars and milled using an oscillatory ball mill (Mixer Mill MM301, Retsch and Co., Germany) at 4 °C. Processing times (5-60 min), milling frequency (5-25 Hz) and number of stainless steel balls (3-60 with a diameter of 4 mm) were selected using a central composite face centered ...

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Retsch Mixer Mill MM 400. SKU:RET-MM400. The mixer mill MM 400 is a compact versatile bench-top unit, which has been developed specially for dry, wet and cryogenic grinding of small amounts of sample. It can mix and homogenize powders and suspensions in only a few seconds. It is also perfectly suitable for the disruption of biological cells as ...

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The raw material of famotidine form B powder (water content: 0.07%, w/w) was respectively ground for 30 min in an oscillatory ball mill (Mixer Mill MM301, Retsch & Co., Germany) at an oscillation frequency of 20 Hz. Each 0.2 g form B powder was placed in a 10 ml volume agate milling jar containing two 10 mm diameter agate balls.

These mixer mills grind, mix, or homogenize 2 samples from 0.2 ml up to 20 ml in a single operation or process up to 20 samples for cell disruption. Mixer Mill MM 200 Range of grinding jars Mixer Mill MM 301 MM 200 MM 301 Sample volume max. 2 x 10 ml 2 x 20 ml Feed grain size max. 6 mm 8 mm Final fineness down to < 10 µ 5 m< m

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BM was performed in an oscillatory ball mill (Mixermill MM400, Retsch & Co., Haan, Germany) at 30 Hz for 90 min in a cold room (5 °C). After milling for 90 min, the amorphized salt-forming samples (confirmed by XRPD and FTIR, the results are shown as Figure S1 and S3 in the supplementary information) were collected and immediately used as ...

Oscillatory ball mill (Mixer Mill MM301, Retsch, Haan, Germany) Indomethacin – – Correlation between physical stability and relaxation time was established for the same amorphous systems prepared by different methods: Oscillatory ball mill (Mixer Mill MM301, Retsch, Haan, Germany) Phenytoin, ibuprofen, salbutamol sulfate – –

RETSCH is the world leading manufacturer of laboratory ball mills and offers the perfect product for each application. The High Energy Ball Mill E max and MM 500 were developed for grinding with the highest energy input. The innovative design of both, the mills and the grinding jars, allows for continuous grinding down to the nano range in the shortest amount of time - with …

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Drug samples (600 mg) were placed in 25 mL stainless steel jars and milled using an oscillatory ball mill (Mixer Mill MM301, Retsch and Co., Germany) at 4 °C. Processing times (5-60 min), milling frequency (5-25 Hz) and number of stainless steel balls (3-60 with a diameter of 4 mm) were selected using a central composite face centered ...

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Subsequently, samples were pulverized using a ball mill (Mixer Mill, MM301; Retsch and Co. Haan, Germany) in order to get very fine and homogeneous plant material. We applied a chemical digestion followed by a colorimetric analysis, as the gravimetric approach has been proven to show a poor reproducibility (Herbauts et al., 1994).

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Drug samples (600 mg) were place d in 25 mL stainless steel jars and mil led using an oscillatory ball mill (Mixer Mill MM301, Retsch and Co., Germany ) …

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A total mass of 500 mg was added into 25 mL ball milling jars with two 12 mm stainless steel balls, and then ball milled in an oscillatory ball mill (Mixermill MM400, Retsch & Co., Haan, Germany) at 30 Hz in a cold lab (5 °C). The ball milling jars were sealed with parafilm to prevent moisture absorption during the BM process.

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